Expertise

Experimental and analytical expertise

A workflow-based overview of synthesis, structural characterization, physical-property measurements, catalysis studies, and data interpretation.

Synthesis and crystal growth

  • Single-crystal growth of halide perovskites and related low-dimensional phases
  • Solid-state synthesis and solution-based synthesis
  • Halide double perovskites and Mo(III)-based halide materials
  • Layered and low-dimensional materials
  • Transition-metal dichalcogenides and related nanocomposites

Structural and compositional characterization

  • Single-crystal X-ray diffraction
  • Powder X-ray diffraction
  • Structure solution and refinement using Olex2, SHELXL, APEX4, and WinGX
  • Crystallographic visualization using Mercury and VESTA
  • Raman spectroscopy, XPS, and EDS-based composition analysis

Physical-property measurements

  • Optical absorption and band-gap analysis
  • UV-Vis diffuse reflectance spectroscopy
  • Magnetic measurements using SQUID and VSM magnetometry
  • Low-temperature magnetic transitions
  • Magnetic exchange and Curie-Weiss analysis

Catalysis-related studies

  • Hydrogen evolution reaction (HER)
  • Photocatalytic hydrogen production studies
  • Electrocatalytic hydrogen production studies
  • MoS2, MoSe2, MoTe2, WS2, and Mo2C-based systems
  • Activity comparison across phase, composition, and interface design

Data analysis and interpretation

  • Structure-property correlations in inorganic and hybrid materials
  • Crystallographic analysis of dimensionality, symmetry, and bond metrics
  • Magnetic, optical, and catalytic data interpretation
  • Origin, Fityk, GSAS-II, and crystallographic figure preparation
  • Research manuscripts, posters, and scientific presentations